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Chapter 9Shape

Powders and ceramics

These processes build solid parts from powders or liquids instead of melting metal or cutting a block. They all rely on sintering: heating packed particles below their melting point until they bond into one solid. What changes from one process to the next is how the particles are shaped, and how heat and pressure are applied.

The big idea

Sintering is how particles stick together without melting. Where two particles touch, atoms drift across the contact point (diffusion) and build a solid bridge, called a neck. As necks grow, the gaps between particles (pores) shrink, so the part gets denser and usually a little smaller. Think of a bowl of snowballs left overnight: they never melt, yet by morning they have fused into one lump. Pressure speeds this up by pushing particles together; fast or internal heating saves time and keeps the tiny crystals fine.

Side by side

ProcessIn one lineBest forBatch sizePrecision
9.1Powder metallurgy (press and sinter)Press powder in a die, then sinter in a belt furnaceSmall gears, bushings, simple-outline parts10,000 to millions a yearAbout ±0.05–0.1 mm
9.2Metal injection molding (MIM)Mold a powder-and-binder paste, remove the binder, sinterTiny, complex, nearly dense steel parts10,000 to millions a yearAbout ±0.3–0.5% of a dimension
9.3Hot isostatic pressing (HIP)Squeeze with hot argon from all sides to close poresCritical castings, printed parts, powder in cansOne part to full furnace loadsShape kept; only pores shrink
9.4Spark plasma sintering (SPS)Pulsed current heats a pressed graphite die in minutesHard ceramics and new materials as discsOne-offs, small batchesRough; ground afterward
9.5Microwave sinteringMicrowaves heat the part from withinCeramics such as dental zirconiaLab work to small batchesLike other sintering, about ±0.5–1%
9.6Sol-gel processingA liquid sets into a gel, then is dried and firedThin coatings, aerogels, pure powdersSingle samples to coating linesFilms to tens of nanometers

How to choose within this family

  • Need hundreds of thousands of simple metal parts cheaply: press-and-sinter powder metallurgy.
  • Need small, complex metal parts that are nearly fully dense: metal injection molding.
  • Need to remove hidden pores from a casting or 3D print that must not fail: hot isostatic pressing.
  • Need a dense disc of a hard-to-sinter or new material, fast: spark plasma sintering, or microwave sintering for ceramics without pressure.
  • Need a thin, pure coating or an ultra-light material: sol-gel processing.

Key words

Sintering
bonding packed particles by heating them below their melting point.
Neck
the solid bridge that grows where two particles touch.
Diffusion
atoms slowly drifting through a solid; it is what builds the necks.
Porosity
the share of a part's volume that is empty pores.
Green part
a shaped part before sintering, held together only weakly.
Binder
a wax or plastic that holds powder in shape until it is removed.
Density
how much of a part is solid material; 100% means no pores.
Shrinkage
the size a part loses as its pores close during sintering.

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